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两段逆流浸出从铁捕集物中富集铂族金属的研究

Study on Enrichment of Platinum Group Metals in Iron-Trapping Material Using Two-Stage Countercurrent Leaching

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【作者】 童伟锋董海刚吴晓峰赵家春李博捷吴跃东保思敏杨海琼

【Author】 TONG Weifeng;DONG Haigang;WU Xiaofeng;ZHAO Jiachun;LI Bojie;WU Yuedong;BAO Simin;YANG Haiqiong;Kunming Institute of Precious Metals, State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals,Sino-Platinum Metals Co. Ltd.;

【机构】 昆明贵金属研究所贵研铂业股份有限公司稀贵金属综合利用新技术国家重点试验室

【摘要】 对熔炼铁捕集物采用两段逆流浸出工艺富集铂族金属进行研究。结果表明,在铁捕集物粉粒度为–0.425 mm,一段浸出温度为常温,浸出硫酸浓度为1.7~1.8 mol/L,固液比(S:L)=1:10,反应时间为0.5 h;二段浸出温度为75℃,浸出硫酸浓度为2 mol/L,S:L=1:50,反应时间为4 h。经此两段浸出后,铂族金属的平均富集倍数为70.6,铂族金属回收率大于99.8%。

【Abstract】 The enrichment process of platinum group metals(PGMs) in the PGM-bearing iron-trapping material was investigated by using the "two-stage countercurrent leaching" technology. When particle size of iron-trapping material was –0.425 mm, the experimental condition for the first stage leaching was room temperature, sulfuric acid concentration of 1.7~1.8 mol/L, solid and liquid ratio(S:L) of 1:10 and leaching for 0.5 h, while that for the second stage leaching was 75℃, sulfuric acid concentration of 2 mol/L, solid and liquid ratio of 1:50 and leaching for 4 h. After two stages leaching, PGMs were enriched about 70.6 times in the iron-trapping material and at least 99.8 % of PGMs could be recovered.

【基金】 国家高技术研究发展(863)计划项目(2012AA063203)
  • 【分类号】TF833
  • 【被引频次】2
  • 【下载频次】207
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