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往复挤压纯镁的组织演变和力学性能

Microstructure and Mechanical Property of Pure Magnesium Processed by Cyclic Extrusion Compression

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【作者】 董婷婷王渠东郭炜刘鉴锋蒋海燕

【Author】 DONG Tingting;WANG Qudong;GUO Wei;LIU Jianfeng;JIANG Haiyan;National Engineering Research Center of Light Alloy Net Forming,Shanghai Jiao Tong University;State Key Laboratory of Metal Matrix Composites,Shanghai Jiao Tong University;

【机构】 上海交通大学轻合金精密成型国家工程研究中心上海交通大学金属基复合材料国家重点实验室

【摘要】 研究了纯镁在350℃往复挤压2,4,8道次,以及在250℃,350℃,450℃往复挤压2道次的组织和力学性能的变化规律。结果表明,纯镁经350℃往复挤压后,组织显著细化,挤压道次从2增加到8时,晶粒尺寸无明显变化,而屈服强度下降,延伸率提高。通过电子背散射衍射技术(EBSD)发现纯镁在350℃往复挤压2,4,8道次后,形成{}0001基面与挤压方向分别约成25°,30°,40°夹角的织构,且织构强度增加,基面滑移系的Schmid因子上升。纯镁在250℃,350℃,450℃往复挤压2道次后,随着挤压温度下降,晶粒尺寸减小,屈服强度上升,屈服强度和晶粒尺寸之间的关系可表述为σs=5.4+338.6d-12。

【Abstract】 Microstructure and tensile property of pure magnesium processed by cyclic extrusion-compression(CEC) at 350℃ for 2, 4 and 8 passes respectively, as well as for 2 passes at 250℃, 350℃ and450℃ respectively are investigated. Results showed that the microstructure of pure magnesium is significantly refined and recrystallized after CEC for 2 passes at 350℃. With the increase of passes, the grain sizes of CECed pure magnesium showed no obvious differences. It was found by means of electron backscatter diffraction(EBSD) analysis that a texture with the basal plane of grains inclining 20o-40o to the extrusion direction developed during the CEC processing. With the increase of CEC passes, the maximum intensity of the texture and Schmid factor of basal slip system increased. Compare to that for 2 passes,the yield stress of pure magnesium after CEC for 8 passes at 350℃ decreases from 60 MPa to 41 MPa,and the elongation increases from 8% to 16.7%. The yield stress and grain size of the pure Mg processed by CEC for 2 passes at 250℃, 350℃and 450℃ follows the Hall-Petch relationship, which can be described as σs= 5.4 + 338.6d-12.

【基金】 国家自然科学基金(51074106,51374145,51404151);中国博士后科学基金2014M561466;上海市博士后科研资助计划14R21411000;资助项目及上海市科学技术委员会资助项目09JC1408200~~
  • 【文献出处】 材料研究学报 ,Chinese Journal of Materials Research , 编辑部邮箱 ,2015年08期
  • 【分类号】TG379
  • 【被引频次】8
  • 【下载频次】263
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