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柿蒂挥发油成分的GC-MS分析

Analysis of Volatile Constituents of Diospyros kaki by GC-MS

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【作者】 陈义高玉琼霍昕杨迺嘉刘建华

【Author】 CHEN Yi;GAO Yu-qiong;HUO Xin;YANG Nai-jia;LIU Jian-hua;Guizhou Base of Biotechnology Research and Development;Guizhou Province Key Lab of Chemistry for Natural Products,Chinese Academy of Sciences;

【机构】 贵州省生物技术研究开发基地贵州省中国科学院天然产物化学重点实验室

【摘要】 目的:研究柿蒂的挥发油成分。方法:采用水蒸气蒸馏法提取柿蒂的挥发油,采用气相色谱-质谱(GC-MS)联用技术对其挥发性成分进行分析,用峰面积归一化法计算各成分的质量分数。结果:共分离出83个化学成分,鉴别出62个化学成分,占挥发油总量的86.704%,其主要成分为己醛(6.465%)、植酮(4.647%)、氧化芳樟醇(4.361%)、壬醛(3.879%)、α-松油醇(3.768%)、2-茨酮(3.519%)、芳樟醇(2.966%)、水菖蒲烯(2.930%)等。结论:GC-MS联用技术可快速、准确地鉴别柿蒂的挥发油成分,可为柿蒂的综合开发和利用提供基础数据。

【Abstract】 OBJECTIVE:To study the volatile constituents of Diospyros kaki. METHODS:The volatile oil was extracted from persimmon calyx by steam distillation. The chemical constituents were analyzed by GC-MS. The mass fraction of the constituents was calculated by peak area normalization method. RESULTS:83 chemical constituents were separated and 62 of them were identified,which accounted for 86.704% of the volatile oil. The major constituents were hexanal(6.465%),phytone(4.647%),linalool oxide(4.361%),nonanal(3.879%),α-terpineol(3.768%),2-bornanone(3.519%),linalool(2.966%)and calarene(2.930%). CONCLUSIONS:GC-MS can identify the volatile oil of D. kaki rapidly and accurately,and can provide basic data for comprehensive utilization of D. kaki.

  • 【分类号】R284.1
  • 【被引频次】2
  • 【下载频次】171
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