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固相微萃取-气质联用分析沙茶酱香气物质的研究

Determination of Aroma Substance in Sha-cha Sauce by Headspace Solid Phase Microextraction and GC/MS

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【作者】 张晓珊陈图锋陈耀文高文华

【Author】 ZHANG Xiao-shan;CHEN Tu-feng;CHEN Yao-wen;GAO Wen-hua;Center Laboratory of Analysis and Testing of Shantou University;

【机构】 汕头大学分析测试中心

【摘要】 目的用顶空固相微萃取-气质联用技术分析沙茶酱中的香气物质。方法优化萃取纤维种类、萃取时间及萃取温度,确定了较佳的萃取条件,进行质谱分析及检索。结果共检测到42种化合物,主要有茴香脑、芳樟醇、烯丙基甲基硫醚、二烯丙基二硫醚等。结论顶空固相微萃取-气质联用可用于沙茶酱中香气物质的快速分析。

【Abstract】 Objective To determine the aroma substances in sha-cha sauce by headspace solid phase microextraction(HS-SPME) and GC/MS. Methods The extraction conditions, including SPME fibers, extraction time and temperature, were optimized. After the optimum condition was selected, the aroma substances were determined by GC-MS, and the MS data were retrieved. Results Forty-two compounds were identified, such as p-propenylanisole, linalool, allyl methyl sulfide, diallyl disulphide, and so on. Conclusion The results showed that HS-SPME-GC-MS can be used in rapid analysis of aroma substances in sha-cha sauce.

【基金】 广东省教育厅科技创新项目(2013KJCX0078);广东省自然科学基金资助项目(S2011010005208)
  • 【分类号】O657.63;TS264.24
  • 【被引频次】6
  • 【下载频次】152
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