节点文献
氰烯菌酯的合成方法改进
Improvement on Synthesis of Phenamacril
【摘要】 以苯甲腈、氰乙酸乙酯等为起始原料,经加成、缩合反应2步合成氰烯菌酯。通过提纯,产品质量分数达到95.0%,总收率大于72%。改进后的方法与原方法相比,线路缩短,易于工业化生产。
【Abstract】 A novel synthetic method was studied. Using benzonitrile, ethyl cyanoacetate as starting materials, phenamacril was obtained by addition and condensation reaction. The purity of the product was 95.0% and the total yield was more than 72%. Compared with the original synthetic method, the novel method was simple and could be used in industry.
【基金】 国家“十二·五”科技支撑计划(2011BAE06B01-11)
- 【文献出处】 现代农药 ,Modern Agrochemicals , 编辑部邮箱 ,2014年06期
- 【分类号】TQ455.4
- 【被引频次】4
- 【下载频次】377