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连续流动注射法测定海水淡化排放水中挥发酚

Determination of Volatile Phenolics in Brine Discharged from Desalination by FIA

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【作者】 曾兴宇刘静潘献辉胡莹莹王燕

【Author】 ZENG Xing-yu;LIU Jing;PAN Xian-hui;HU Ying-ying;WANG Yan;Institute of Seawater Desalination and Multipurpose Utilization,SOA;National Marine Environmental Monitoring Center;

【机构】 国家海洋局天津海水淡化与综合利用研究所国家海洋环境监测中心

【摘要】 采用连续流动注射法测定海水淡化排放水中的挥发酚。优化了浓盐水体系中连续流动注射分光光度法测定挥发酚的条件。在0.0μg/L~75.0μg/L浓度范围内线形关系良好,线性相关系数r为0.999 91,方法的检出限为0.35μg/L,相对标准偏差为0.70%~2.17%,平均回收率为100.05%~101.2%。方法快速、简便,能满足海水淡化浓盐水中挥发酚定量测定要求。

【Abstract】 It was developed a method for FIA determination of volatile phenolics in brine discharged from desalination. The instrument conditions were optimized. The linear correlation coefficient at concentrations ranging from 0. 0 μg / L to 75. 0 μg / L was 0. 99991. The detection limit of this method was 0. 35 μg / L. The relative standard deviation( RSD%) for the determination of volatile phenolics in brine discharged from desalination was 0. 07% ~ 2. 17% and the recovery was 100. 05% ~ 101. 2%. The method was simple and rapid for the determination of volatile phenolics in brine discharged from desalination.

【关键词】 连续流动注射海水淡化浓盐水挥发酚
【Key words】 FIAdesalinationbrinevolatile phenolics
【基金】 海洋公益性行业科研专项经费项目(201305039);中央级公益性科研院所基本科研业务费专项资金项目(K-JBYWF-2011-G23)
  • 【文献出处】 盐业与化工 ,Journal of Salt and Chemical Industry , 编辑部邮箱 ,2014年05期
  • 【分类号】P747
  • 【被引频次】3
  • 【下载频次】101
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