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PVP保护下纳米银颗粒的液相化学还原法制备及表征

Synthesis and Characterization of Silver Nano-particles by Liquid Phase Chemical Deoxidization Method under the Protection of PVP

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【作者】 王春霞李英琳徐磊

【Author】 WANG Chunxia;LI Yinglin;XU Lei;School of Textiles, Tianjin Polytechnic University;School of Materials Science and Engineering, Tianjin Polytechnic University;

【机构】 天津工业大学纺织学院天津工业大学材料科学与工程学院

【摘要】 以PVP为表面活性剂,甲酸铵为还原剂,采用液相还原法制备了纳米银颗粒。采用X射线衍射(XRD)、透射电子显微镜(TEM)和紫外-可见光吸收光谱(UV-Vis)对所制备样品进行表征。结果显示:当PVP与Ag NO3的质量比为2.2:1,陈化时间24 h,得到立方块和六棱柱的银混合颗粒。

【Abstract】 Nano-silver particles were prepared by using polyvinyl pyrolidone as the dispersing agent and ammonium as the reducing agent. The resulting specimens were characterized by X-ray diffraction(XRD), transmission electron microscopy(TEM) and UV-Vis adsorption spectrum. The result revealed that a mixture of cube and hexagonal prisms of nano-silver particles was obtained when the mass ratio of PVP to Ag NO3 was 2.2:1 and the aging time was 24 hours.

【基金】 天津工业大学青年教师基金项目(029986)
  • 【分类号】TB383.1
  • 【被引频次】10
  • 【下载频次】617
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