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PVP保护下纳米银颗粒的液相化学还原法制备及表征
Synthesis and Characterization of Silver Nano-particles by Liquid Phase Chemical Deoxidization Method under the Protection of PVP
【摘要】 以PVP为表面活性剂,甲酸铵为还原剂,采用液相还原法制备了纳米银颗粒。采用X射线衍射(XRD)、透射电子显微镜(TEM)和紫外-可见光吸收光谱(UV-Vis)对所制备样品进行表征。结果显示:当PVP与Ag NO3的质量比为2.2:1,陈化时间24 h,得到立方块和六棱柱的银混合颗粒。
【Abstract】 Nano-silver particles were prepared by using polyvinyl pyrolidone as the dispersing agent and ammonium as the reducing agent. The resulting specimens were characterized by X-ray diffraction(XRD), transmission electron microscopy(TEM) and UV-Vis adsorption spectrum. The result revealed that a mixture of cube and hexagonal prisms of nano-silver particles was obtained when the mass ratio of PVP to Ag NO3 was 2.2:1 and the aging time was 24 hours.
【关键词】 纳米化学;
纳米银;
化学还原法;
PVP;
陈化时间;
【Key words】 nanochemistry; nano-particles; chemical reduction method; PVP; aging time;
【Key words】 nanochemistry; nano-particles; chemical reduction method; PVP; aging time;
【基金】 天津工业大学青年教师基金项目(029986)
- 【文献出处】 贵金属 ,Precious Metals , 编辑部邮箱 ,2014年04期
- 【分类号】TB383.1
- 【被引频次】10
- 【下载频次】617