【摘要】 采用三聚氰胺为原料一步合成目标产物三聚氰胺二硝酸盐(MDN)。利用红外光谱、核磁共振、元素分析等手段对产物的结构进行了表征,反应得率为52.7%。研究了反应温度和反应时间对反应的影响,确定了最佳反应条件为反应时间1h,反应温度95℃。更多还原

【Abstract】 A novel energetic compound melaminium dinitrate(MDN) was synthesized using melamine as starting material.The structure of product were characterized by using infrared spectrum,nuclear magnetic resonance,element analysis,and so on. The yield of this reaction was 52.7 %. The influence of reaction temperature and time on reaction yield was investigated. The optimal reaction conditions were defined as follows: reaction time is 1h,reaction temperature is 95 ℃.更多还原