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新型可降解Mg-1Ca合金微弧氧化工艺初探

Fabrication and Characterization of Micro-arc Oxidation(MAO) Coatings on Novel Biodegradable Mg-1Ca Alloy for Orthopaedic Application

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【作者】 贾昭君李明刘倩徐旭晨成艳郑玉峰奚廷斐魏世成

【Author】 Jia Zhaojun;Li Ming;Liu Qian;Xu Xuchen;Cheng Yan;Zheng Yufeng;Xi Tingfei;Wei Shicheng;Academy for Advanced Interdisciplinary Studies, Peking University;College of Engineering, Peking University;School and Hospital of Stomatology, Peking University;

【机构】 北京大学前沿交叉学科研究院北京大学工学院北京大学口腔医学院

【摘要】 采用微弧氧化(Micro-arc oxidation,MAO)在镁合金表面制备一层多孔陶瓷膜可以有效改善基体的耐蚀性和生物相容性。文章以新型Mg-1Ca为基体进行微弧氧化处理,研究了处理时间和电压对MAO膜层结构和成分及耐蚀性的影响,讨论了膜层的生长机理及其在SBF溶液中的腐蚀行为。

【Abstract】 A newly-developed degradable Mg-1Ca(mass fraction%) alloy was modified with porous ceramic coatings through Micro-arc oxidation(MAO) technique in alkaline silicate electrolyte. The sparking behavior and growth characteristics of oxide coatings were discussed. The influence of working voltage and treatment time on the the resulting coatings’ structure and composition were investigated by SEM-EDS, XPS and XRD. Potentiodynamic polarization test was carried out to understand corrosion behavior of the coated Mg-1Ca in Kokubo’s SBF solution, in which the optimal MAO treatment at 360 V for 5 min was determined.

【基金】 国家自然科学基金(31370954);生物电子学国家重点实验室开放研究基金
  • 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2014年S1期
  • 【分类号】TG174.4
  • 【被引频次】5
  • 【下载频次】190
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