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K403镍基铸造合金热暴露后的微观组织与性能

Microstructure and Properties of K403 Nickel Based Alloy After Thermal Exposure

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【作者】 刘君孙志超唐文亭

【Author】 LIU Jun 1,2,SUN Zhi-chao 1,TANG Wen-ting 2(1.State Key Laboratory of Solidification Processing,Northwestern Polytechnical University,Xi’an 710072,Shaanxi,China;2.School of Materials Science and Engineering,Xi’an University of Technology,Xi’an 710048,Shaanxi,China)

【机构】 西北工业大学凝固技术国家重点实验室西安理工大学材料科学与工程学院

【摘要】 采用扫描电镜研究了K403镍基铸造高温合金在850℃下,热暴露50~200 h后的微观组织,并分析了力学性能的变化。结果表明:热暴露前后的组织均为典型的树枝晶组织,热暴露后(γ+γ′)相共晶特征趋于不明显,MC碳化物部分发生分解,在枝晶间、晶界附近和碳化物周围析出有害的TCP脆性相即针状σ相,并且随着热暴露时间的延长,针状σ相析出量增多;合金的名义屈服强度和抗拉强度随热暴露时间的延长而下降,硬度略有提高,塑性降低;针状的σ脆性相的析出是导致合金力学性能下降的主要原因之一。

【Abstract】 The microstructure of Ni-based casting superalloy K403 after thermal exposure at 850 ℃ for 50-200 h were studied by SEM.And the mechanical properties were also analyzed.The results show that the microstructure of the alloy presents a typical dendritic structure before and after thermal exposure.However,after the thermal exposure,(γ+γ′)eutectic phase feature is not evident,and the part of MC carbides have decomposed,while the harmful TCP brittle phase namely acicular σ phase are also precipitated in the interdendritic regions,the grain boundary and the carbide surrounding,and with the prolonging time of the thermal exposure,acicular σ phase precipitation increases.With increasing the time,the offset yielding stress and tensile strength were reduced,while the hardness was improved slightly and the plasticity was reduced.The acicular σ brittle phase precipitation was one of the main reasons for the deterioration of alloy mechanical properties.

【基金】 国家自然科学基金重点项目(50935007);国家“973”课题(2010CB731701);西安市科技计划项目(CX12180-8)
  • 【分类号】TG136.1
  • 【被引频次】5
  • 【下载频次】218
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