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马肾果叶的化学成分研究
Chemical constituents from leaves of Aglaia testicularis
【摘要】 研究马肾果叶的化学成分。采用硅胶、Sephadex LH-20、高效制备液相等方法,对马肾果甲醇提取物进行分离纯化,通过质谱(MS)、波谱数据分析(1H-,13C-NMR)进行结构鉴定。从马肾果甲醇提取物中分离7个化合物,分别鉴定为dasyclamide(1),aglamide A(2),aglamide B(3),aglamide C(4),aglamide D(5),aglaroxin A 1-O-acetate(6),3’-methoxyaglaroxin A1-O-acetate(7)。上述化合物均为首次从该植物中分离得到。
【Abstract】 To study the chemical constituents from the leaves of Aglaia testicularis. The methanol extract was isolated and purified by silica gel,Sephadex LH-20 and preparative HPLC. Their chemical structures were elucidated by MS and spectral data(1H, 13C-NMR). Seven compounds were isolated from the leaves and identified as dasyclamide( 1),aglamide A( 2),aglamide B( 3), aglamide C( 4),aglamide D( 5),aglaroxin A 1-O-acetate( 6),and 3’-methoxyaglaroxin A 1-O-acetate( 7). All compounds were isolated from this plant for the first time.
- 【文献出处】 中国中药杂志 ,China Journal of Chinese Materia Medica , 编辑部邮箱 ,2013年20期
- 【分类号】R284
- 【被引频次】1
- 【下载频次】110