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氯化镁喷雾热解制备氧化镁的研究

Study on preparation of magnesium oxide by spray pyrolysis of magnesium chloride

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【作者】 都永生孙庆国火焱韩继龙李明珍

【Author】 Du Yongsheng,Sun Qingguo,Huo Yan,Han Jilong,Li Mingzhen(Laboratory of Salt Lake Resources and Chemistry,Qinghai Institute of Salt Lakes,Chinese Academy of Sciences,Xining 810008,China)

【机构】 中国科学院青海盐湖研究所盐湖资源与化学实验室

【摘要】 以青海盐湖氯化镁为初级原料,氯化镁经溶解、除杂、精制后采用喷雾热解法在立式热解炉中热解制备氧化镁。着重研究了喷雾热解的温度和进料量对氯化镁分解率的影响,最终确定的最佳工艺条件为:喷雾热解制备氧化镁时氯化镁的最佳热解温度为600℃,进料量为12 L/h。最佳工艺条件下氯化镁分解率在99%以上。该方法工艺流程简单、便于操作,是一种很有应用前景的氧化镁生产方法。

【Abstract】 Magnesium oxide was prepared with magnesium chloride from Qinghai Salt Lake as the primary raw material.Through dissolving,purification,and refining,the magnesium chloride was pyrolyzed by spray pyrolysis method in a vertical pyrolysis furnace to prepare magnesium oxide.Influence of temperature and feed rate on the decomposition rate of magnesium chloride was emphatically studied,and the optimum conditions were confirmed:the best pyrolysis temperature was 600 ℃ and feed rate was 12 L/h.Under the optimum conditions,the decomposition rate of magnesium chloride was more than 99%.The advantage of this method was simple,and easy to operate,therefore it′s a promising production method of magnesium oxide.

【基金】 中国科学院知识创新工程重要方向项目(KZCX2-YW-343)
  • 【文献出处】 无机盐工业 ,Inorganic Chemicals Industry , 编辑部邮箱 ,2013年04期
  • 【分类号】TQ132.2
  • 【被引频次】20
  • 【下载频次】417
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