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卡尔费休容量滴定法测定血管封合剂的水分含量
Determination of the Moisture Content in Vascular Sealant by Karl Fischer Volumetric Titration Method
【摘要】 验证了卡尔费休容量法对血管封合剂水分含量测定的准确性和可靠性。标准工作曲线的线性相关系数r=0.9999,检出限为0.075 mg。采用加标回收率,实验结果为回收率97.19%~99.62%。对同一样品平行测定6次,相对标准偏差为3.66%。
【Abstract】 To verify the accuracy and reliability of Karl Fischer volumetric method of vascular Sealant moisture content measurement.The linear correlation coefficient of standard working curve was 0.9999.The detection limit of this method was 0.075mg.The results were obtained by using the recovery which were 97.19%~99.62%.The same samples were parallel determined by 6 times,and the relative standard deviation was 3.66%.
【关键词】 卡尔费休容量滴定法;
血管封合剂;
水分含量;
线性相关系数;
回收率;
【Key words】 Karl Fischer volumetric titration method; Vascular sealant; Moisture content; Linear correlation coefficient; Recovery;
【Key words】 Karl Fischer volumetric titration method; Vascular sealant; Moisture content; Linear correlation coefficient; Recovery;
- 【文献出处】 生物医学工程研究 ,Journal of Biomedical Engineering Research , 编辑部邮箱 ,2013年01期
- 【分类号】R927.2
- 【下载频次】64