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利用热脱附/冷阱捕集提取土壤中挥发性有机物的条件研究
Optimal Conditions for Extraction of the VOCs in Soil by Thermal Desorption-Cold Trap
【摘要】 采用热脱附/冷阱捕集提取土壤中的挥发性有机物,以17种VOCs作为目标研究对象进行挥发性有机物的提取条件研究。试验确定的提取条件为:热脱附温度300℃,热脱附时间3 min,冷阱捕集温度–10℃。优化条件后添加水平为1 mg/kg的加标土壤样品测定结果在0.75~0.94 mg/kg之间,相对标准偏差为2.89%~7.16%。
【Abstract】 Volatile organic compounds(VOCs) in soil were extracted by thermal desorption-cold trap,and the extraction conditions were researched with 17 VOCs as objective.The extraction conditions determined through the experiments were as the following: thermal desorption temperature was 300℃,thermal desorption time was 3 min,and the cold trap temperature was –10℃.In these conditions,1 mg/kg standard was added in samples,and the determination results were between 0.75 and 0.94 mg/kg,and the relative standard deviations were 2.89% –7.16%.
【关键词】 土壤;
挥发性有机物;
热脱附/冷阱捕集;
提取;
【Key words】 soil; volatile organic compounds(VOCs); thermal desorption-cold trap; extraction;
【Key words】 soil; volatile organic compounds(VOCs); thermal desorption-cold trap; extraction;
【基金】 广西科学基金项目(桂科青0991045)
- 【文献出处】 化学分析计量 ,Chemical Analysis and Meterage , 编辑部邮箱 ,2013年02期
- 【分类号】X833;O657.63
- 【被引频次】5
- 【下载频次】164