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CdSe量子点的合成及其对潜指纹的荧光显现研究

Synthesis of CdSe Quantum Dots and Their Applications for Labeling of Latent Fingerprints

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【作者】 许尊炼伊魁宇马子宁王猛刘显峰

【Author】 XU Zun-lian1,YI Kui-yu1,MA Zi-ning1,WANG Meng2,LIU Xian-feng1 (1Department of Forensic Chemistry,China Criminal Police College,Shenyang 110035,Liaolin,China; 2 Department of Trace Examination,China Criminal Police College,Shenyang 110035,Liaolin,China)

【机构】 中国刑警学院法化学系中国刑警学院痕迹检验技术系

【摘要】 以水热法在水相中直接合成了巯基乙酸修饰的CdSe量子点,并将合成的CdSe量子点进行表征、纯化。在波长365 nm紫外光的激发下,CdSe量子点发射出明亮的黄绿色荧光,荧光发射峰约位于528nm,将得到的CdSe量子点纳米发光材料应用于非渗透性客体上潜指纹的荧光标记成像研究,发现CdSe量子点溶液显现的手印纹线流畅,显现细节特征明显,呈现明亮的黄绿色荧光指纹,具有很高的实用价值和鉴定价值。

【Abstract】 Thioglycolic acid(TGA) capped water-soluble CdSe quantum dots(QDs) was synthesized via a hydrothermal synthesis method.The as-prepared QDs were characterized and purified.Thioglycolic acid(TGA) capped water-soluble CdSe quantum dots emitted strong yellow-green light under the irradiation of UV light at the wavelength of 365 nm,and the PL emission peak is at about 528 nm.Finally,the prepared thioglycolic acid capped CdSe quantum dots were applied in the fluorescent labeling of latent fingerprints on the surface of smooth objects.It is found the fingerprint details on the surface of smooth objects were clearly developed,detail characteristic is obvious,and the bright yellow-green fluorescence fingerprint was developed clearly.It has very high practical value and the value of identification.

【基金】 国家自然科学基金项目(21205139);公安部应用创新计划项目(2012YYCXXJXY127);中国刑事警察学院大学生创新训练计划项目(201210175033)资助
  • 【文献出处】 合成材料老化与应用 ,Synthetic Materials Aging and Application , 编辑部邮箱 ,2013年02期
  • 【分类号】O657.3;O614.242
  • 【被引频次】1
  • 【下载频次】176
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