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微波辅助酸改性粉煤灰处理含砷废水

Treatment of Arsenic-containing Wastewater with Microwave-assisted Acid Modified Fly-ash

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【作者】 缑星刘德汞曹珍曹书勤

【Author】 GOU Xing,LIU Degong,CAO Zhen,CAO Shuqin(College of Chemistry and Chemical Engineering,Xinyang Normal University,Xinyang 464000,China)

【机构】 信阳师范学院化学化工学院

【摘要】 以浓度1.0mol.L-1的硫酸为改性剂,微波辅助制备酸改性粉煤灰吸附剂.通过SEM,FTIR对粉煤灰微观形貌观察及结构表征,用分光光度法对其吸附性能进行分析,结果表明:用硫酸用量为4g.mL-1、微波功率400W、微波时间8min时制得的酸改性粉煤灰来处理含砷废水,常温下,当吸附剂用量10g.L-1,废水pH=6,吸附时间30min时,砷的脱除率可达90.29%.

【Abstract】 Acid modified fly ash was prepared through microwave-assisted with 1.0 moL·L-1 sulfuric acid.We observe its microstructure by SEM and FTIR to its structure and index and aualyze of the adsorption performance by spectrophotometry.The result shows that:under the modified conditions with the dosage of sulphate acid 4 mL·g-1,microwave power 400 W,modification time 8 min and with the adsorption conditions of the mass of adsorbent 10 g·L-1,waste water pH=6,adsorption time 30 min,temperature 25 ℃,the removal rate of arsenic reach to 90.29%.

【基金】 河南省科技攻关项目(0624240012)
  • 【文献出处】 河南师范大学学报(自然科学版) ,Journal of Henan Normal University(Natural Science Edition) , 编辑部邮箱 ,2013年03期
  • 【分类号】X703
  • 【被引频次】10
  • 【下载频次】187
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