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2,4-二氯苯酚液相色谱分析
Determination of 2,4-Dichlorophenol by HPLC
【摘要】 建立一种采用高效液相色谱法测定2,4-二氯苯酚的定量分析方法,选用甲醇+水作流动相,RP-18色谱柱,检测波长254 nm,外标法定量。本方法的回收率在98.1%~101.8%,标准偏差0.225,变异系数1.98%。2,4-二氯苯酚得到较好分离,操作简便、实用,本方法定量分析结果准确、稳定。
【Abstract】 The chromatographic column was packed with RP-18 and the methanol and water was applied as mobile phase,the 2,4-Dichlorophenol was determined by HPLC.The detection wave length was at 254 nm,the standard deviation was 0.225,the variation coefficients was 1.98%,and the recovery was between 98.1% ~ 101.8%.
- 【文献出处】 广州化工 ,Guangzhou Chemical Industry , 编辑部邮箱 ,2013年23期
- 【分类号】O657.72
- 【被引频次】3
- 【下载频次】427