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拉曼光谱及其检测时样品前处理的研究进展

Research Progress in Raman Spectra and Its Test Sample Pretreatment

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【作者】 韦娜冯叙桥张孝芳齐小花邹明强王明泰

【Author】 WEI Na1,2,FENG Xu-qiao2,ZHANG Xiao-fang1,QI Xiao-hua1,ZOU Ming-qiang1,WANG Ming-tai3 1.Chinese Academy of Inspection and Quarantine,Beijing 100123,China 2.Shenyang Agricultural University,Shenyang 110161,China 3.Inspection and Quarantine Technology Center,Jinlin Entry-Exit Inspection and Quarantine Bureau,Jinlin 130062,China

【机构】 中国检验检疫科学研究院沈阳农业大学吉林出入境检验检疫局检验检疫技术中心

【摘要】 拉曼光谱具有操作简单,所需样本量小,检测灵敏度高等特点,可进行现场快速筛查、检测及鉴别。样品前处理直接影响分析结果的准确度和精密度,而且操作繁琐费时。发展快速、高效的样品前处理技术进而结合拉曼光谱检测技术具有重要的研究意义,特别是与增强拉曼光谱相结合进行食品、农产品中等残留物的衡量检测已成为研究热点。本文阐述了拉曼光谱产生的原理,介绍了拉曼光谱的起源和发展,讨论了表面增强拉曼光谱技术、针尖增强拉曼光谱技术和壳层隔绝纳米粒子增强拉曼光谱技术,并对拉曼检测之前的样品预处理进行了讨论。

【Abstract】 It is generally accepted that Raman spectroscopy is an advanced method with simple operation,small amount of specimens needed as well as rapid on-line screening,detection and identification.However,in the technology of determination,sample preparation is also an significant factor during analysis process.It would affect the accuracy and precision of the results,and normally involved complicated procedure.Developing a rapid and effective sample preparation method coupled with Raman detective technology is a method worth study.In the present paper,the simply basic principle,the origin and development of generating Raman spectra were introduced,some Raman technology,such as the surface-enhanced Raman spectroscopy,tip-enhanced Raman spectroscopy,shell-isolated nanoparticle enhanced Raman spectroscopy and the sample preparation were discussed.

【基金】 “十二五”支撑计划项目(2012BAK25B01,2012BAK08B06-1);吉林省世行贷款农产品质量安全项目(2011-Z48)资助
  • 【文献出处】 光谱学与光谱分析 ,Spectroscopy and Spectral Analysis , 编辑部邮箱 ,2013年03期
  • 【分类号】O657.37
  • 【被引频次】52
  • 【下载频次】3662
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