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微波消解-ICP-AES法测定飞机草不同部位常量与微量元素含量

DETERMINATION OF CONSTANT AND TRACE ELEMENTS IN DIFFERENT PARTS OF EUPATORIUMODORATUM L.BY MICROWAVE DIGESTION-ICP-AES

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【作者】 杨茹梁国兴王彩芳何兰

【Author】 YANG Ru;LIANG Guoxing;WANG Caifang;HE Lan;College of Chemistry,Beijing Normal University;School of Pharmaceutical Sciences,Zhengzhou University;

【机构】 北京师范大学化学学院郑州大学药学院

【摘要】 用硝酸、高氯酸、过氧化氢(体积比3∶3∶4)作消解剂,采用微波消解处理样品,建立了电感耦合等离子体发射光谱法(ICP-AES)同时测定飞机草茎(主干和嫩枝)、根(主根和须根)及叶各部位中Ca、Mg、Na、Fe、Mn、Zn、Al、Ba、B、Cr、Cu、Sr、Ti 13种常量与微量元素含量.结果显示飞机草各部位元素分布有较大差异,大多数元素在根和叶中含量较多.

【Abstract】 A method based on microwave digestion and inductively coupled plasma-atomic emission spectrometry(ICP-AES)was established for simultaneous determination of thirteen constant and trace elements(Ca,Mg,Na,Fe,Mn,Zn,Al,Ba,B,Cr,Cu,Sr and Ti)in stems,roots and leaves of Eupatorium odoratum L..Samples were digested in microwaved mixture of HNO3,HClO4and H2O2(3∶3∶4).Optimal conditions for microwave digestion and working parameter of ICP-AES were obtained.It was found that these elements were present in plant parts at different levels,most were present more in roots and in leaves.

【基金】 公益性行业(农业)科研专项资金资助项目(201103027);“重大新药创制”科技重大专项资金资助项目(2011ZX09307-002-01)
  • 【文献出处】 北京师范大学学报(自然科学版) ,Journal of Beijing Normal University(Natural Science) , 编辑部邮箱 ,2013年05期
  • 【分类号】S451
  • 【下载频次】83
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