节点文献
微波法提取断肠草生物总碱的工艺
Microwave-Assisted Extraction Techniques for the Total Alkaloid of Gelsemium Elegans Benth
【摘要】 利用微波辅助萃取技术提取断肠草生物总碱,以其生物总碱粗提率为指标,考察不同提取条件下的提取率.结果表明:以氯仿作为提取溶剂、微波功率500 W、料液比1∶8.0、提取时间360s(120 s×3)时生物总碱得率最高为1.63%,生物总碱提取率显著提高.
【Abstract】 Using the microwave-assisted extraction techniques for the total alkaloid of Gelsemium Elegans Benth and analyzing the extraction yield,this research focused on the different experimental conditions for such extraction.The result showed that using CHCl3 as solvent,the microwave power at 500 W,the solid-to-liquid ratio at 1∶ 8.0,the extraction time for 360 s(120 s for each,3 times),the experiment had the highest yield of 1.63% and the extraction yield for the total Alkaloid improved remarkably.
【关键词】 断肠草;
生物总碱;
微波提取;
正交实验;
【Key words】 Gelsemium elegans Benth; total alkaloids; microwave-assisted extraction; orthogonal experiment;
【Key words】 Gelsemium elegans Benth; total alkaloids; microwave-assisted extraction; orthogonal experiment;
【基金】 国家自然科学基金(30960460);云南省自然科学基金((2007B0006Z)
- 【文献出处】 云南民族大学学报(自然科学版) ,Journal of Yunnan University of Nationalities(Natural Sciences Edition) , 编辑部邮箱 ,2012年02期
- 【分类号】TQ461
- 【被引频次】1
- 【下载频次】171