【摘要】 目的:建立盆炎清灌肠剂的质量控制标准。方法:采用薄层色谱法检测制剂中的丹参、三棱、红藤和乌药;用高效液相色谱法测定制剂中丹酚酸B的提取量。结果:定性鉴别分离度好,专属性好;丹酚酸B进样量为0.0422～0.2532 mg/ml范围内与峰面积呈良好的线性关系,y=8620485.78x-9724.5(r=0.9997,n=6),测得制剂中的丹酚酸B含量稳定。结论:所建立的方法稳定可靠,准确,专属性好,可用于制剂的质量控制。更多还原

【Abstract】 Objective: TO built the standard of Pen YanQin enemas′quilty controling.Method :Adopting the TLC to test the Salvia miltiorrhiza Bunge、Sparganium stdoniferum Buch.-Ham.、Sargentodoxa Cuneata(Oliv.)Rehd.et Wils、Lindera aggregata(Sims)Kosterm in the preparation,then using the HPLC to test the extraction of Salvianolic Acid B.Result: Qualitative identification had good separation and specificity,and Sal B and the injection volume was within the range of 0.0422～0.2532 mg/ml peakarea showed a good linear relationship,y=8620485678x-9724.5(r=0.9997,n=6),Preparations measured concentration in the stability of Sal B.Conclusion: The method is reliable,accurate and specific and can be used to control the quality.更多还原