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锦灯笼酸浆宿萼皂苷提取工艺的研究
Extraction Process of Saponins from Physalis alkekengi Calyx
【摘要】 以锦灯笼酸浆宿萼为原料,采用回流提取工艺研究了乙醇浓度、浸提时间、浸提温度和料液比对皂苷得率的影响。在单因素试验的基础上进行了正交试验,得到最优提取工艺组合为:80%的乙醇,60℃,120min,1∶9的料液比。此条件下总皂苷的得率为4.283mg.g-1。由方差分析可得,时间对皂苷提取率的影响差异不显著,故可缩短时间至105min。
【Abstract】 This study focused on the influences of ethanol concentration,extraction time,extraction temperature and liquid-solid ratio on the yield of total saponins from dried Physalis alkekengi calyx powder.Results of orthogonal test showed that the yield of saponins reached 4.283 mg·g-1 by using 80%(v) ethanol as solvent,liquid-solid ratio 9∶1 and temperature 60℃.Results of variance analysis showed that extraction time was non-significant at 5% probability level,so it can be shortened to 105 min.
【基金】 山西省科技攻关项目(20100311073)
- 【文献出处】 山西农业大学学报(自然科学版) ,Journal of Shanxi Agricultural University(Natural Science Edition) , 编辑部邮箱 ,2012年04期
- 【分类号】TQ914
- 【被引频次】5
- 【下载频次】331