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低温热处理对Graphit-iC类石墨碳膜组织结构及耐磨性的影响
EFFECT OF LOW TEMPERATURE HEAT TREATMENT ON STRUCTURE AND WEAR BEHAVIOR OF GRAPHIT-iC GRAPHITE-LIKE CARBON COATINGS
【摘要】 应用拉曼光谱(Raman)等测试方法分析了不同热处理温度对PVD技术制备的Graphit-iC类石墨碳膜涂层的组织结构、显微硬度、结合强度和磨损率的影响规律。结果表明:随温度升高,涂层发生sp3→sp2结构转变,相对强度比I_D/I_G增加,石墨化倾向增大;涂层磨损率在25~250℃温度区间内保持较低的水平,当温度继续上升后表面显微硬度及结合力降低,磨损率显著增大,耐磨性降低。
【Abstract】 The effects of heat treatment temperature on microstructure,micro-hardness,wear and adhesion strength of Graphit-iC graphite-like carbon coatings prepared by PVD technique were analyzed by Raman spectroscopy and other test.The results indicated that as temperature increasing, sp3→sp2 phase transition was observed in the coatings and the intensity ratio I_D/I_G increased,and the tendency of graphitization was obvious.The wear rate maintained at low level between the temperature of 25~250℃,although the wear rates of the coatings increased obviously as the temperature increased,the micro-hardness and coating-substrate adhesion strength decreased.
【Key words】 Graphit-iC Graphite-Like Carbon Coatings; Low Temperature Heat Treatment; Microstructure; Wear;
- 【文献出处】 上海金属 ,Shanghai Metals , 编辑部邮箱 ,2012年04期
- 【分类号】TG174.44
- 【被引频次】1
- 【下载频次】89