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50%醚菌酯水分散粒剂的研制

Preparation of Kresoxim-methyl 50% Water Dispersible Granules

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【作者】 刘勇良周磊张宗俭张春华卢忠利

【Author】 LIU Yong-liang1,ZHOU Lei3,ZHANG Zong-jian1,2,ZHANG Chun-hua1,2,LU Zhong-li1,2(1.Beijing Grand AgroChem Co.,Ltd.,Beijing 100083,China;2.Central Academe of Chinese Chemical Science and Technology,Beijing 100083,China;3.Chemical and Engineering College,China University of Mining and Technology,Beijing 100083,China)

【机构】 北京广源益农化学有限责任公司中国矿业大学化学与工程学院中化化工科学技术研究总院

【摘要】 [目的]研制出各项性能指标合格的50%醚菌酯水分散粒剂。[方法]以制剂悬浮率和崩解性为考察指标,对分散剂、润湿剂、崩解剂及填料进行筛选。[结果]50%醚菌酯水分散粒剂最佳配方(以质量分数计):有效成分质量分数为96%的醚菌酯52%,分散剂GY-D800 6%、助分散剂GY-SN02 10%、润湿剂GY-WS01 3%、崩解剂氯化钠10%、填料为高岭土18%、黏结剂为水。[结论]对制剂性能指标检测,结果表明该产品的崩解分散性好,热贮前悬浮率为91.0%,6次崩解,持久泡沫量为0,热贮(54±2)℃,14 d后悬浮率为83.3%,5次崩解,持久起泡性量为0,有效成分热贮分解率3.2%,各项指标均符合国标要求。

【Abstract】 Kresoxim-methyl 50% water dispersible granules was prepared,and the performance index of the formulation was qualified.[Methods] The dispersing agent,wetting agent,disintegrating agent and packing were selected in the method of testing the suspension rate and disintegrative.[Results] Kresoxim-methyl(96% purity) 52%,GY-D800 6% as dispersing agent,GY-SN02 10% as assistant dispering agent,GY-WS01 3% as wetting agent,NaCl 10% as disintegrating agent,kaolin 18% as packing,water as binder were formulated into an optimum formulation of kresoxim-methyl 50% water dispersible granules.[Conclusions] The result of formulation test showed that the granules had good disintegration and dispersibility.Suspension rate was 91.0%,disintegration was 6 times,lasting foaming amount was 0.After thermal storage at(54±2) °C for 14 d,the suspension rate was 83.3%,disintegration was 5 times,lasting foaming amount was 0,effective components decomposition rate was 3.2%,all specifications were fit for the requirement of GB.

【基金】 十二五”国家科技支撑计划(2011BAE06A06);国家高技术研究发展计划(863计划)(2011AA10A201)
  • 【分类号】TQ450.6
  • 【被引频次】8
  • 【下载频次】179
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