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溶胶—凝胶法制备莫来石—氧化硅—顽火辉石复合纤维
Preparation of Mullite-Silica-Enstatite Composites Fibers with Sol-gel Method
【摘要】 用硝酸铝、氧化镁和正硅酸乙酯为原料,乳酸为络合剂,用溶胶—凝胶法制备了莫来石—氧化硅—顽火辉石复合纤维。用FTIR、XRD和SEM对凝胶纤维和陶瓷纤维进行表征。结果表明,凝胶纤维在1 200℃煅烧2h后得到了具有光滑表面和致密微观结构的莫来石—氧化硅—顽火辉石复合纤维。
【Abstract】 Mullite-silica-enstatite composites fibers were prepared with sol-gel method with aluminum nitrate,magnesia and tetraethyl orthosilicate as raw materials,and lactic acid as complexant.FTIR spectra,XRD,and SEM analysis were applied to characterize the properties of the gel and ceramic fibers.The results show that the composites fibers with a smooth surface and dense microstructure are obtained through the sintering gel fibers at 1 200 ℃ for 2 h.
【关键词】 莫来石—氧化硅—顽火辉石复合材料;
纤维;
溶胶—凝胶法;
【Key words】 mullite-silica-enstatite composites; fibers; sol-gel method;
【Key words】 mullite-silica-enstatite composites; fibers; sol-gel method;
【基金】 陕西省自然科学基金项目(2012JQ6017);陕西理工学院基金项目(SLGQD1101)
- 【文献出处】 有色金属(冶炼部分) ,Nonferrous Metals(Extractive Metallurgy) , 编辑部邮箱 ,2012年11期
- 【分类号】TQ174.1
- 【被引频次】1
- 【下载频次】113