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脉冲磁场处理Fe52Co34Hf7B6Cu1非晶的低温真空退火效应

EFFECT OF LOW-TEMPERATURE VACUUM ANNEALING ON THE MAGNETIC PULSED AMORPHOUS Fe52Co34Hf7B6Cui ALLOY

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【作者】 晁月盛王莉张艳辉朱涵娴罗丽平

【Author】 CHAO Yuesheng,WANG Li,ZHANG Yanhui,ZHU Hanxian,LUO Liping College of Sciences,Northeastern University,Shenyang 110819

【机构】 东北大学理学院

【摘要】 对Fe52Co34Hf7B6Cu1非晶合金进行了低频磁脉冲处理,研究低温真空退火对磁脉冲处理Fe52Co34Hf7B6Cu1非晶软磁性能的影响.结果表明,磁脉冲处理导致非晶合金发生纳米晶化,析出晶态相α-Fe(Co),晶粒尺寸为5-10 nm,形成的纳米晶粒弥散分布于非晶基体的双相纳米合金中.对磁脉冲处理的试样进行低温真空退火,可以进一步优化纳米合金的软磁性能,在100℃退火可以得到最佳的软磁性能.

【Abstract】 The nanocrystalline Fe52Co34Hf7B6Cu1 soft magnatic alloys composed of bcc-Fe nanocrystals embedded in a residual amorphous matrix were obtained by the magneto-crystallization of melt-spun ribbons.In order to improve the soft magnetic properties of double-phase Fe(Co)-based nanocrystalline alloy,the nanocrystalline alloy specimens were vacuum annealed for 30 min at 100, 200 and 300℃.The results showed that the treatment of magnetic pulsing on the amorphous alloy resulted in the nanocrystallization,the grain size of precipitatedα-Fe(Co) nanocrystallized phase was 5—10 nm.The low-temperature vacuum annealing of magnetic pulsed specimens further improved the soft magnetic properties of nanocrystalline alloy.The influence of annealing at 100℃for 30 min on the properties is most obvious.

【基金】 国家自然科学基金资助项目50771025~~
  • 【文献出处】 金属学报 ,Acta Metallurgica Sinica , 编辑部邮箱 ,2012年06期
  • 【分类号】TG156.2
  • 【被引频次】2
  • 【下载频次】147
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