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脉冲磁场处理Fe52Co34Hf7B6Cu1非晶的低温真空退火效应
EFFECT OF LOW-TEMPERATURE VACUUM ANNEALING ON THE MAGNETIC PULSED AMORPHOUS Fe52Co34Hf7B6Cui ALLOY
【摘要】 对Fe52Co34Hf7B6Cu1非晶合金进行了低频磁脉冲处理,研究低温真空退火对磁脉冲处理Fe52Co34Hf7B6Cu1非晶软磁性能的影响.结果表明,磁脉冲处理导致非晶合金发生纳米晶化,析出晶态相α-Fe(Co),晶粒尺寸为5-10 nm,形成的纳米晶粒弥散分布于非晶基体的双相纳米合金中.对磁脉冲处理的试样进行低温真空退火,可以进一步优化纳米合金的软磁性能,在100℃退火可以得到最佳的软磁性能.
【Abstract】 The nanocrystalline Fe52Co34Hf7B6Cu1 soft magnatic alloys composed of bcc-Fe nanocrystals embedded in a residual amorphous matrix were obtained by the magneto-crystallization of melt-spun ribbons.In order to improve the soft magnetic properties of double-phase Fe(Co)-based nanocrystalline alloy,the nanocrystalline alloy specimens were vacuum annealed for 30 min at 100, 200 and 300℃.The results showed that the treatment of magnetic pulsing on the amorphous alloy resulted in the nanocrystallization,the grain size of precipitatedα-Fe(Co) nanocrystallized phase was 5—10 nm.The low-temperature vacuum annealing of magnetic pulsed specimens further improved the soft magnetic properties of nanocrystalline alloy.The influence of annealing at 100℃for 30 min on the properties is most obvious.
【Key words】 amorphous alloy; magnetic pulsing; two-phases nanocrystalline alloy; lowtemperature vacuum annealing; magnetic property;
- 【文献出处】 金属学报 ,Acta Metallurgica Sinica , 编辑部邮箱 ,2012年06期
- 【分类号】TG156.2
- 【被引频次】2
- 【下载频次】147