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Synthesis and Crystal Structure Analysis of 2-Amino-4,6-bis(diphenoxyl phosphoramide)-1,3,5-triazine

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【作者】 张楠成昌梅王如骥

【Author】 ZHANG Nan a CHENG Chang-Mei a WANG Ru-Ji b a (Key Laboratory of Bioorganic Phosphorus Chemistry & Chemical Biology (Ministry of Education), Department of Chemistry, Tsinghua University, Beijing 100084, China) b (Tsinghua University, Beijing 100084, China)

【机构】 Key Laboratory of Bioorganic Phosphorus Chemistry & Chemical Biology (Ministry of Education),Department of Chemistry,Tsinghua UniversityTsinghua University

【摘要】 A disubstituted triazine compound, namely, 2-amino-4,6-bis(diphenoxyl phosphorramide)-1,3,5-triazine, which is an inherent flame retardant monomer, was synthesized specifically, and its structure was characterized by using NMR spectrum and X-ray single-crystal diffraction. Unit cell parameters: space group P21/c, Z=4, a=8.7494(15), b=27.518(5), c=12.511(2),β=109.323(16) , Z=4, V=2842.7(9)β3 , Dc=1.380 g/cm3 , F(000)=1224 and Mr=590.46. All the atoms are in the general positions.

【Abstract】 A disubstituted triazine compound, namely, 2-amino-4,6-bis(diphenoxyl phosphorramide)-1,3,5-triazine, which is an inherent flame retardant monomer, was synthesized specifically, and its structure was characterized by using NMR spectrum and X-ray single-crystal diffraction. Unit cell parameters: space group P21/c, Z=4, a=8.7494(15), b=27.518(5), c=12.511(2),β=109.323(16) , Z=4, V=2842.7(9)β3 , Dc=1.380 g/cm3 , F(000)=1224 and Mr=590.46. All the atoms are in the general positions.

  • 【文献出处】 结构化学 ,Chinese Journal of Structural Chemistry , 编辑部邮箱 ,2012年07期
  • 【分类号】O626
  • 【下载频次】72
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