【摘要】 以1-甲基咪唑,溴乙烷和乙酸铅为原料,采用"一锅法"合成了离子液体1-乙基-3-甲基咪唑醋酸盐,产率87%,其结构经UV,IR和元素分析确证。优化反应条件为:1-甲基咪唑100 mmol,n(溴乙烷):n(1-甲基咪唑):n(乙酸铅)=3.6:2.0:1.0,于60℃反应20 h。更多还原

【Abstract】 A ionic liquid,1-ethyl-3-methylimidazolium acetate in yield of 87%,was synthesized by one-pot method from 1-methylimidozole,bromethyl and lead acetate.The structure was confirmed by UV,IR and elemental analysis.The optimal reaction conditions at 60 ℃ for 20 h were as follows:1-methylimidazole was 100 mmol,n(bromethyl):n(1-methylimidazole):n(lead acetate) was 3.6:2.0:1.0.更多还原