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类水滑石的制备及表征
Preparation and Characterization of Hydrotalcite-Like Compound
【摘要】 采用低饱和共沉淀法制备Zn-Al LDHs、Mg-Al LDHs、Co-Al LDHs系列水滑石,通过X射线衍射(XRD)、傅里叶红外光谱(FT-IR)、热重-差热分析(TG-DTA)等表征手段对上述样品进行分析和表征。结果表明:采用低饱和共沉淀法制备的上述水滑石结晶度较高,结构规整,具有良好的层状结构和热稳定性。
【Abstract】 The Zn-Al LDHs、Mg-Al LDHs and Co-Al LDHs powders were prepared with low-super-saturation-co-precipitation method.The presented samples were characterized in detail by X-ray diffraction(XRD),infrared spectroscopy(FT-IR) and thermo-gravimetric differential thermal analysis(TG-DTA).The results showed that the above series of hydrotalcite by low-super-saturation-co-precipitation possessed high crystallinity,overall plan,good layered structure and thermal properties.
【基金】 贵州大学自然科学青年科研基金[2009(064)]
- 【文献出处】 贵州化工 ,Guizhou Chemical Industry , 编辑部邮箱 ,2012年01期
- 【分类号】O643.32
- 【被引频次】8
- 【下载频次】381