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柑橘皮渣总黄酮提取工艺研究

Study on the Extraction Process for Total Flavonoids in Orange Peel

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【作者】 李辰梁硕赵燕黄俊添

【Author】 Li Chen1,2,Liang Shuo1,Zhao Yan2,Huang Juntian1(1.Morden Agriculture Development Ltd.,of Xinhui,Jiangmen 529100; 2.Instrumental Analysis & Research Center,Wuyi University,Jiangmen 529020,China)

【机构】 江门市新会区现代农业发展有限公司五邑大学分析测试中心

【摘要】 以超声波提取法优选柑橘皮渣总黄酮提取工艺。采用L9(34)正交实验法,以浸膏得率(%)和浸膏中总黄酮含量(%)为评价指标,考察物料比(g∶mL)、乙醇含量(%)、提取时间(min)和提取温度(℃)对柑橘皮渣总黄酮提取的影响。结果表明以20倍量70%乙醇于50℃下超声提取40 min,提取2次为最佳提取工艺。该优选的工艺条件可提高柑橘皮渣综合利用率,并为制备高附加值柑橘产品提供一定参考。

【Abstract】 The optimum extraction process conditions for total flavonoids from orange peel was investingated using ultrasonic wave method.The extraction rate(%) of ethanol extractum and content of total flavonoids(%) were chosen as the assessment index by using the L9(34) orthogonal design.The solvent quantum to orange peel(g∶mL),ethanol content(%),extraction time(min) and extraction temperature(℃) were reviewed.The optimum ethanol extraction process conditions were as follows: adding 20 fold of 70 % ethanol,extracting for 40 min at 50 ℃,and extracting two times.The optimum extraction process can give a reference to the research of multiple utilization and preparation of high additive valuable products from orange peel.

【关键词】 柑橘皮总黄酮提取正交试验
【Key words】 orange peeltotal flavonoidsextractionorthogonal design
【基金】 江门市科技计划项目(江计划科[2011]042)
  • 【文献出处】 广东化工 ,Guangdong Chemical Industry , 编辑部邮箱 ,2012年05期
  • 【分类号】TQ461
  • 【下载频次】296
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