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黄杞叶挥发油化学成分的GC-MS分析

GC-MS Analysis of Chemical Components of Volatile Oil from Leaves of Engelhardtia roxburghiana

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【作者】 胡东南蒋才武黄健军

【Author】 HU Dong-nan1,JIANG Cai-wu2,HUANG Jian-Jun2*(1.Guangxi Botanical Garden of Medicinal Plant,Nanning 530023,China; 2.Institute of Chinese Materia Medica,Guangxi Traditional Chinese Medical University,Nanning 530001,China)

【机构】 广西壮族自治区药用植物园广西中医学院中药研究所

【摘要】 目的:研究黄杞叶的挥发油成分。方法:采用水蒸气蒸馏法提取黄杞叶中的挥发油,并通过气相色谱-质谱(GC-MS)联用仪对其化学成分进行分析和鉴定,用色谱峰面积归一化法计算各组分相对百分含量。结果:从黄杞叶挥发油中共分离出55个组分,鉴定了其中33个化合物,占总量的95.0%,主要成分为十六烷酸(hexadecanoic acid,44.73%)、叶绿醇(phytol,14.71%)、十八碳-9,12,15-三烯醛(9,12,15-octadecatriena,12.24%)等。结论:分析结果可为黄杞叶的质量控制提供依据,并为提高黄杞叶的进一步开发利用提供参考。

【Abstract】 Objective:To analyze the volatile oil from the leaves of Engelharditia roxburghiana.Method: The volatile oil was extracted from leaves of E.roxburghiana by steam distillation,the amount of the components from the volatile oil was separated and identified by GC-MS,and the relative content of each component was calculated by area normalization method.Result: Fifty five compounds were separated by GC and 33 of them were identified,which accounted for 95% of volatile oil.The major components were hexadecanoic acid(44.73%),phytol(14.71%),9,12,15-octadecatriena(12.24%) et al.Conclusion: The analysis results can provide evidence for quality control and further exploitation of leaves of E.roxburghiana.

【关键词】 黄杞挥发油气相质谱-质谱
【Key words】 Engelhardtia roxburghianavolatile oilGC-MS
  • 【文献出处】 中国实验方剂学杂志 ,Chinese Journal of Experimental Traditional Medical Formulae , 编辑部邮箱 ,2011年21期
  • 【分类号】R284.1
  • 【被引频次】8
  • 【下载频次】156
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