【摘要】 等物质的量的苯磺酰胺钠盐与异硫氰酸酯在封管中、无溶剂和130℃条件下反应,得到一系列苯磺酰硫脲衍生物,产率高到中等.产物结构通过IR,¹H NMR,¹³C NMR,ESI-MS和元素分析的表征.更多还原

【Abstract】 A series of benzenesulfonylthioureas were synthesized by the reaction of sodium benzenesulfamides and isosulfocyanates in sealed tube at 130℃and solvent-free conditions in moderate to good yields.All products were characterized by IR,¹H NMR,¹³C NMR,ESI-MS techniques and elemental analysis.更多还原