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水热还原法制备铜

Preparation of Copper under Hydrothermal Condition

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【作者】 任鑫帮赵莲花

【Author】 REN Xin-bang,ZHAO Lian-hua~* (Department of Chemistry,College of Science,Yanbian University,Yanji 133002,China)

【机构】 延边大学理学院化学系

【摘要】 以CuSO4·H2O为原料,葡萄糖为还原剂,采用水热法成功制备出铜。并川X射线衍射(XRD)和扫描电镜(SEM)对其结构和形貌进行了表征。结果表明:当OH-、Cu2+、葡萄糖的摩尔比为4:3:1,水热温度为160℃,反应时间为24 h时,产物为无规则形貌的铜;当加入离子液体时,产物的平均粒径为5.1μm的球形铜。

【Abstract】 Copper was prepared by hydrothermal process using cupric suifate pentanhydrate as raw materials and glucose as reducing agent.It’s structure and morphology was characterized by X-ray diffraction(XRD) and scanning electron microscopy(SEM).When the molar ratio of OH,Cu2+,glucose was 4:3:1 in the reaction precursor,temperature was 160 C and the reaction time was 24 h.copper of irregular morphology was obtained. Futhermore when used ionic liquid,the product became spherical,it’s average particle size was 5.1μm.

  • 【文献出处】 延边大学学报(自然科学版) ,Journal of Yanbian University(Natural Science Edition) , 编辑部邮箱 ,2011年04期
  • 【分类号】O614.121
  • 【下载频次】135
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