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光度法快速测定化妆品中甲醛

Rapid Determination of Formaldehyde in Cosmetics by Spectrophotometry

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【作者】 宋佳刘瓘文

【Author】 SONG Jia 1,2 LIU Guanwen 1,2 (1.Shanghai Research Institute of Fragrance & Flavor Industry,Shanghai 200232,China;2.Shanghai Daily Chemical Industrial Research Institute,Shanghai 200232,China)

【机构】 上海香料研究所上海市日用化学研究所

【摘要】 光度法测定甲醛,灵敏度高、选择性好、成本较低,但对化妆品样品的前处理时间较长。目前用光度法快速测定化妆品中甲醛的方法尚未见报道。用乙酰丙酮作显色剂,提高反应速率,以50%异丙醇作测定溶液,即能解决样品前处理时间长的缺陷。甲醛的方法检测限为0.78mg/L。回收率范围95%~97%,RSD为0.5186%~2.0032%。方法精密度高,准确度好,测定速度快,可用于商业化妆品中甲醛的快速测定。与标准检测方法进行比对,结果满意(Z=0.35)。

【Abstract】 Determination of formaldehyde by spectrophotometer is a method with high sensitivity,good selectivity and low cost,but the pre-treatment of samples for cosmetics is longer.Rapid Determination of formaldehyde in cosmetics by this method has not been reported so far.The method here is as follows: using acetyl acetone reagent to accelerate the reaction rate,50% isopropyl alcohol solution was used as detection solution,which can solve the longer sample preparation times problem.The detection limit for formaldehyde was 0.78 mg/L,recoveries were 95% ~ 97%,RSD was between 0.5186% ~ 2.0032%.The method is high precision,good accuracy,quick and can be used for commercial rapid determination of formaldehyde in cosmetics.The method and the standard detection methods were compared,the satisfactory results(Z = 0.35) were obtained.

  • 【文献出处】 香料香精化妆品 ,Flavour Fragrance Cosmetics , 编辑部邮箱 ,2011年04期
  • 【分类号】TQ658
  • 【被引频次】5
  • 【下载频次】219
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