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壮药依肝达颗粒质量标准研究
Quality Standard for Yigangda Granules
【摘要】 目的建立壮药依肝达颗粒的质量标准。方法采用薄层色谱法进行定性鉴别,以高效液相色谱法测定槲皮素的含量。结果薄层色谱分离度好,专属性强。槲皮素的线性范围为0.058~0.58μg(r=0.999 8,n=6),平均回收率为103.82%,RSD=0.84%(n=6)。结论所建立的方法简便、准确、专属性强、重复性好,可有效控制壮药依肝达颗粒的质量。
【Abstract】 Objective To establish the quality standard for Yiganda Granules. Methods TLC was used for qualitative identification.The content of quercetin was determined by HPLC. Results The result of TLC was separable and specific.The standard curve was linear in the range of 0.058~0.58 μg(r=0.999 8,n =6) for quercetin.The average recovery was 103.82%(RSD= 0.84%,n =6). Conclusion The method is simple,accurate,specific,reproducible and can be applied to the quality control of Zhuangyao Yiganda Granules.
【基金】 国家“十一五”科技支撑计划课题(No.2006BAI06A17-03)
- 【文献出处】 时珍国医国药 ,Lishizhen Medicine and Materia Medica Research , 编辑部邮箱 ,2011年11期
- 【分类号】R286.0
- 【被引频次】1
- 【下载频次】99