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电感耦合等离子体原子发射光谱法测定面粉中铅和镉

ICP-AES Determination of Lead and Cadmium in Flour

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【作者】 李志富胡作林

【Author】 LI Zhi-fu~1,HU Zuo-lin~2 (1.Dept.of Chem.and Chem.Eng.,Taishan Medical College,Tai’an 271016,China; 2.Tai’an Municipal Center for Prevention and Control of Disease,Tai’an 271000,China)

【机构】 泰山医学院化学与化学工程学院泰安市疾病预防控制中心

【摘要】 :采用电感耦合等离子体原子发射光谱法测定面粉中痕量铅和镉。面粉用乙醇和硝酸溶解后,加入分散剂Triton X-80溶液得到样品的悬浊液。然后经均质器分散10 min后,在磁力搅拌下搅拌8 min动态进样分析。铅和镉的检出限(3S/N)分别为0.05,0.006 mg·L-1,加标平均回收率分别为98.8%,96.7%。

【Abstract】 A method of ICP-AES for the determination of Pb and Cd in flour was proposed.Flour was dissolved with ethanol and HNO3,and Triton X-80 solution was added as dispersing agent.The suspension obtained was dispersed with homogenizer for 10 min and agitated with magnetic stir for 8 min,then introduced into the instrument for analysis.Values of detection limits of the method were 0.05 mg·L-1 and 0.006 mg·L-1 and values of recovery found were 98.8%and 96.7%for Pb and Cd respectively.

【基金】 泰山医学院科研基金资助项目(2009ZR010)
  • 【文献出处】 理化检验(化学分册) ,Physical Testing and Chemical Analysis(Part B:Chemical Analysis) , 编辑部邮箱 ,2011年03期
  • 【分类号】TS211.7
  • 【被引频次】5
  • 【下载频次】150
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