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电感耦合等离子体原子发射光谱法测定面粉中铅和镉
ICP-AES Determination of Lead and Cadmium in Flour
【摘要】 :采用电感耦合等离子体原子发射光谱法测定面粉中痕量铅和镉。面粉用乙醇和硝酸溶解后,加入分散剂Triton X-80溶液得到样品的悬浊液。然后经均质器分散10 min后,在磁力搅拌下搅拌8 min动态进样分析。铅和镉的检出限(3S/N)分别为0.05,0.006 mg·L-1,加标平均回收率分别为98.8%,96.7%。
【Abstract】 A method of ICP-AES for the determination of Pb and Cd in flour was proposed.Flour was dissolved with ethanol and HNO3,and Triton X-80 solution was added as dispersing agent.The suspension obtained was dispersed with homogenizer for 10 min and agitated with magnetic stir for 8 min,then introduced into the instrument for analysis.Values of detection limits of the method were 0.05 mg·L-1 and 0.006 mg·L-1 and values of recovery found were 98.8%and 96.7%for Pb and Cd respectively.
【关键词】 电感耦合等离子体原子发射光谱法;
悬浮液进样;
面粉;
铅;
镉;
【Key words】 ICP-AES; Suspension sample introduction; Flour; Lead; Cadmium;
【Key words】 ICP-AES; Suspension sample introduction; Flour; Lead; Cadmium;
【基金】 泰山医学院科研基金资助项目(2009ZR010)
- 【文献出处】 理化检验(化学分册) ,Physical Testing and Chemical Analysis(Part B:Chemical Analysis) , 编辑部邮箱 ,2011年03期
- 【分类号】TS211.7
- 【被引频次】5
- 【下载频次】150