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鹿茸骨宝胶囊质量标准的研究

Quality Standard for Luronggubao Capsule

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【作者】 李庆杰王全凯博士儒常艳茹赵昱玮杨丽刘永强

【Author】 LI Qing-jie1,WANG Quan-kai2,BO Shi-ru2,CHANG Yan-ru1,ZHAO Yu-wei1,YANG Li2,LIU Yong-qiang4(1.Jilin Tianyao Technology Co.,Ltd.,Changchun 130012,China;2.College of Chinese Medicinal Materials,Jilin Agricultural University,Changchun 130118,China;3.Inner Mongolia People′s Hospital,Hohhot 010017,China;4.The Affiliated Hospital to Changchun University of Chinese Medicine,Changchun 130117,China)

【机构】 吉林天药科技有限公司吉林农业大学中药材学院内蒙古自治区人民医院中药房长春中医药大学附属医院

【摘要】 为建立鹿茸骨宝胶囊的质量标准,采用薄层色谱法对胶囊中的鹿茸、淫羊藿、槐角进行了定性鉴别;采用高效液相色谱法测定了胶囊中淫羊藿苷含量。结果表明:薄层色谱斑点清晰,空白样品无干扰,可用于本品质量控制;淫羊藿苷在0.051 25~1.025μg范围内具有良好的线性关系r=0.999,平均加样回收率为98.78%,RSD为1.65%(n=6)。说明该方法简便、精确、重现性好,可作为该制剂的质量控制。

【Abstract】 To establish the quality standards of Luronggubao capsule,Cornu Cervi Pantotrichum,Herba Epimedii,Fructus Sophorae in capsule were identified by TLC,Icariin in capsule were determinated by HPLC.The TLC spots were clear,and the control test showed no interference.It can be used for the product quality control.The linear relationship of Icariin was good when Paeoniflorin was at the range of 0.051 25-1.025 μg(r=0.999).The showed recovery was 98.78% and RSD was 1.65%(n=6).The method developed is simple and accurate.It can be used for quality control of the Luronggubao capsule.

【基金】 吉林省科技支撑计划项目(20080916)
  • 【文献出处】 经济动物学报 ,Journal of Economic Animal , 编辑部邮箱 ,2011年01期
  • 【分类号】S865.42
  • 【被引频次】1
  • 【下载频次】91
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