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A Two-dimensional Coordination Polymer of Manganese(II) and Benzimidazole-5,6-dicarboxylate

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【Author】 BI Cheng-Lua, b SUN Jian-Huab② a (School of Chemistry and Environmental Engineering, Jiangsu Teachers University of Technology, Changzhou, Jiangsu 213001, China) b (Jiangsu Province Key Laboratory of Precious Metal Chemistry and Technology, Changzhou, Jiangsu 213001, China)

【机构】 School of Chemistry and Environmental Engineering, Jiangsu Teachers University of Technology, Changzhou； Jiangsu Province Key Laboratory of Precious Metal Chemistry and Technology；

【摘要】 A new two-dimensional (2D) manganese(II) coordination polymer {[Mn(bidc)(H2O)2]· 2H2O}n (H2bidc = benzimidazole-5,6-dicarboxylic acid) was synthesized, and characterized by X-ray crystallography and other measurements. The complex crystallizes in the orthorhombic system, space group Pbca with a = 7.0218(7), b = 17.9701(18), c = 19.0697(19), V = 2406.3(4)3, Z = 8, Dc = 1.823 g/cm3, Mr = 330.14, F(000) = 1344, μ(MoKα) = 1.140 mm-1, S = 1.055, R = 0.0305 and wR = 0.1012 for 2130 observed reflections (I > 2σ(I)). The title complex consists of a novel 2D network with a topology of short symbol (4.82)(4.82).更多还原

【Abstract】 A new two-dimensional (2D) manganese(II) coordination polymer {[Mn(bidc)(H2O)2]· 2H2O}n (H2bidc = benzimidazole-5,6-dicarboxylic acid) was synthesized, and characterized by X-ray crystallography and other measurements. The complex crystallizes in the orthorhombic system, space group Pbca with a = 7.0218(7), b = 17.9701(18), c = 19.0697(19), V = 2406.3(4)3, Z = 8, Dc = 1.823 g/cm3, Mr = 330.14, F(000) = 1344, μ(MoKα) = 1.140 mm-1, S = 1.055, R = 0.0305 and wR = 0.1012 for 2130 observed reflections (I > 2σ(I)). The title complex consists of a novel 2D network with a topology of short symbol (4.82)(4.82).更多还原

【关键词】 manganese； benzimidazole-5； 6-dicarboxylate； crystal structure； coordination polymer；
【Key words】 manganese； benzimidazole-5； 6-dicarboxylate； crystal structure； coordination polymer；

【基金】 supported by the National Natural Science Foundation of China (No. 40743017);the Open Foundation of Jiangsu Key Laboratory of Precious Metals Chemistry (SYGK0706)

【文献出处】结构化学 ,Chinese Journal of Structural Chemistry , 编辑部邮箱 ,2011年08期

【分类号】O633.5
【下载频次】57

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