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晶化温度对敞开体系合成中孔分子筛Ti-MCM-41的影响
Effects of Crystallization Temperature on Ti-MCM-41 Preparing in an Open System
【摘要】 在敞开体系中合成出Ti-MCM-41,利用X射线衍射(XRD)、红外光谱(FT-IR)、紫外-可见光谱(UV-Vis)和孔结构测定对合成样品进行了表征,讨论了晶化温度对中孔分子筛Ti-MCM-41晶化的影响.
【Abstract】 In an open-vessel,the mesoporous molecular sieve Ti-MCM-41 was synthesized.The characterization of synthesized samples was carried out by means of X ray diffraction(XRD),Fourier transform infrared spectrometer(FT-IR),Visiblespectroscopy(UV-Vis) and mensuration of pore structure.The effect of crystallization temperature on the crystallization of the mesoporous molecular sieve was discussed.
【关键词】 中孔分子筛;
晶化温度;
合成;
表征;
【Key words】 mesoporous molecular sieve; crystallization temperature; synthesis; characterization;
【Key words】 mesoporous molecular sieve; crystallization temperature; synthesis; characterization;
【基金】 河南省教育厅自然科学研究计划项目(2009A150007)
- 【文献出处】 河南教育学院学报(自然科学版) ,Journal of Henan Institute of Education(Natural Science Edition) , 编辑部邮箱 ,2011年04期
- 【分类号】TQ424.25
- 【下载频次】67