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不同萃取方法对长江口边滩多环芳烃萃取效果的影响

Effect of extracting methods on the extraction efficiency of PAHs collected from the Yangtze estuarine and coastal areas

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【作者】 张谦栋刘敏欧冬妮杨毅李勇

【Author】 ZHANG Qiandong,LIU Min,OU Dongni,YANG Yi,LI Yong.(Key Laboratory of Geographic Information Science,Ministry of Education,School of Resources and Environment Science,East China Normal University,Shanghai 200062)

【机构】 华东师范大学资源与环境科学学院教育部地理信息科学重点实验室

【摘要】 选取索氏提取法和加速溶剂萃取仪(ASE)提取法,对长江口边滩样品进行多环芳烃萃取实验,并利用气相色谱/质谱仪对萃取出来的多环芳烃进行定量分析,研究了不同萃取方法以及不同溶剂条件下多环芳烃的总量、分布特征。结果表明,长江口边滩多环芳烃最高值出现在吴淞口;索氏提取法在多环芳烃萃取效果上优于加速溶剂萃取仪提取法;混合溶剂萃取效果要优于单一溶剂。

【Abstract】 The sediment samples collected from Yangtze estuarine and coastal areas were extracted by Soxhlet extracting method and accelerated solvent extraction method.The extracted liquids were determined by GC/MS.The effect of extraction method and solvent on the concentration,distribution and types of extracted PAHs were analyzed.The results showed that the highest concentration of PAHs was found at Wusongkou;Soxhlet extracting method was better than accelerated solvent extraction method in the extraction efficiency;mixed solvent presented better performance than single solvent extraction in PAHs extraction.

【基金】 国家自然科学基金资助项目(No.40971268、No.40801201、No.51009068);中国博士后基金资助项目(No.20080440605)
  • 【文献出处】 环境污染与防治 ,Environmental Pollution & Control , 编辑部邮箱 ,2011年10期
  • 【分类号】X832
  • 【被引频次】18
  • 【下载频次】272
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