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氨基甲酸酯型脱氧胆酸分子裂缝的微波合成
Synthesis of Novel Carbamate-type Molecular Clefts Based on Deoxycholic Acid under Microwave Irradiation
【摘要】 在微波辐射条件下,以脱氧胆酸为隔离基,通过三光气桥连各种芳香胺,以良好的产率合成了一系列新的分子裂缝,其结构经1H NMR,IR,MS和元素分析确证。
【Abstract】 A series of novel molecular clefts were synthesized in good yields using deoxycholic acid as spacer to bridge different aromatic amines via triphosgene under microwave irradiation.The structures were confirmed by 1H NMR,IR,MS and elemental analysis.
【关键词】 脱氧胆酸;
分子裂缝;
微波辐射;
合成;
【Key words】 deoxycholic acid; molecular clefts; microwave irradiation; synthesis;
【Key words】 deoxycholic acid; molecular clefts; microwave irradiation; synthesis;
【基金】 国家外专局资助项目(2009-15)
- 【文献出处】 合成化学 ,Chinese Journal of Synthetic Chemistry , 编辑部邮箱 ,2011年02期
- 【分类号】O621.3
- 【被引频次】1
- 【下载频次】75