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微波合成ZnO微米“花”
Microwave Synthesis of ZnO Micrometer Flowers
【摘要】 以硝酸锌为锌源,乙醇胺为矿化剂,水为溶剂,微波加热20min,合成了由微米棒自组装而成的ZnO微米"花"(1),其结构和形貌经X-射线衍射、场扫描电子显微镜和透射电子显微镜表征。结果表明,1由六棱柱形的微米棒自组装而成,微米棒长度1μm~1.5μm,直径300nm~500nm。
【Abstract】 ZnO micrometer flowers(1) with high crystallinity were synthesized using zinc nitrate as the zine source and ethanolamine as the mineralizer and water as the solvent under microwave irradiation for 20 min.The structure and morphology of 1 were characterized by XRD,FESEM and TEM.The experiment results showed that 1 was assembled by hexagonal micrometer rods,which had lengths of 1.0 μm~1.5 μm and diameters of 300 nm~500 nm.
【关键词】 ZnO;
半导体;
微米花;
微波;
合成;
【Key words】 zinc oxide; semiconductor; micrometer flower; microwave; synthesis;
【Key words】 zinc oxide; semiconductor; micrometer flower; microwave; synthesis;
【基金】 国家自然科学基金资助项目(20501002);安徽省第五批优秀青年科技基金资助项目(10040606Y25);安徽省高校优秀青年基金资助项目(2009SQRZ104ZD);合肥学院科研发展基金重点项目(11KY01ZD)
- 【文献出处】 合成化学 ,Chinese Journal of Synthetic Chemistry , 编辑部邮箱 ,2011年01期
- 【分类号】TB383.1
- 【被引频次】1
- 【下载频次】192