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ICP-AES测定青岛崂山绿茶中的微量元素

Determination of Trace Elements in Qingdao Laoshan Tea Leaves by ICP-AES

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【作者】 赵艳芳宁劲松尚德荣翟毓秀

【Author】 ZHAO Yan-Fanga,b NING Jin-Songa,b SHANG De-Ronga,b ZHAI Yu-Xiua,ba(Yellow Sea Fishery Research Institute,Chinese Academy of Fishery Sciences,Qingdao,Shandong 266071,P.R.China)b(The National Center for Quality Supervision and Test of Aquatic Products,Qingdao,Shandong 266071,P.R.China)

【机构】 中国水产科学研究院黄海水产研究所国家水产品质量监督检验中心

【摘要】 采用HNO3-H2O2混合酸,密闭微波消解样品,应用ICP-AES测定青岛崂山绿茶中Al、Ca、Cd、Co、Cr、Cu、Fe、K、Mg、Mn、Na、Ni、Pb、Se、Sr、V和Zn等17种营养元素及重金属元素的含量。测定结果的相对标准偏差均小于3.50%,对17种元素的加标回收率在90.0%—110.2%之间,采用该方法测得的茶叶标准物质(GBW10016)的17种元素的值均在标准值范围内,方法准确度高。实验结果表明青岛崂山绿茶中含有大量对人体有益的元素包括Ca、Co、Cr、Cu、Fe、K、Mg、Mn、Na、Ni、Se、Sr、V和Zn等,另外也检测到含有Al,Cd和Pb等有毒、有害元素,但是含量很低,对人体的不利影响可以忽略不计。

【Abstract】 The 17 kinds of elements,including Al,Ca,Cd,Co,Cr,Cu,Fe,K,Mg,Mn,Na,Ni,Pb,Se,Sr,V and Zn in Laoshan tea leaves were determined by ICP-AES with nitric acid-hydrogen peroxide for sealed microwave digestion.The relative standard derivation was below 3.50%,and the recovery of all elements was in the range of 90.0%—110.2% while all elements of the standard tea(GBW 10016) were all in the range of the criterion,and the method was very accurate.The Laoshan Tea contained large amount of useful elements including Ca,Co,Cr,Cu,Fe,K,Mg,Mn,Na,Ni,Se,Sr,V,Zn,etc.In addition,several harmful elements including Al,Cd and Pb were also detected,the content of which were so low that their affection for human body could be ignored.

【基金】 中国水产科学研究院基本科研业务费(2060302);农业行业标准-钙磷测定(22201015)
  • 【文献出处】 光谱实验室 ,Chinese Journal of Spectroscopy Laboratory , 编辑部邮箱 ,2011年03期
  • 【分类号】O657.31;TS272.7
  • 【被引频次】7
  • 【下载频次】212
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