In this paper,a modified method of DSPE for the determination of 20 pesticide residues in tea was established.These pesticides were BHCs,DDTs,endosulfan,pyrethroid pesticides,acetochlor,fipronil,chlorfenapyr,which were concerned in the tea international trade.The pretreatment procedure was:(1) the target pesticide residues were extracted by 2 mL of pure acetonitrile in 0.5 g of tea,then vortexed by a vortexer vigorously for 2 min and centrifuged for 5 min at 5000 r/min;(2) 1 mL of supernate was mixed with P...