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液相化学还原法制备纳米银及抗菌性能研究

Preparation of Silver Nanoparticles by the Liquid-phase Chemistry Reducing Method and Their Antimicrobial Properties

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【作者】 孔茉莉高冠慧常雪婷尹衍升

【Author】 KONG Moli1,GAO Guanhui1,CHANG Xueting2,YIN Yansheng1,2(1 Institute of Materials Science and Engineering,Ocean University of China,Qingdao 266100;2 Institute of MaterialsScience and Engineering,Shanghai Maritime University,Shanghai 201306)

【机构】 中国海洋大学材料科学与工程研究院上海海事大学材料科学与工程研究院

【摘要】 选用液相化学还原法,分别在以羧甲基纤维素钠(Carboxymethyl cellulose sodium,CMC)和葡萄糖为还原剂的体系下制备纳米银颗粒,并进行了对比分析。通过紫外分光光度计、X射线衍射和透射电镜等测试手段对其进行了表征。结果表明,用CMC体系制备的纳米银粉末平均粒径为20~30nm,为多晶结构;用葡萄糖体系制备的纳米银粉末平均粒径为25~35nm,为面心结构。利用抑菌圈法对纳米银的抗菌性能进行测试,结果显示2种体系下制备的纳米银对海洋芽孢杆菌都有很好的抑制作用。

【Abstract】 The silver nitrate was selected as the silver source,the polyethylene pyrrolidone as stabilizer,carboxymethyl cellulose sodium(CMC) and the glucose as reducing agent separately,the nano-silver was prepared under two different systems using the liquid phase chemistry reducing method.The nano-silver particles were measured through ultraviolet spectrophotometer test,X-ray diffraction and transmission electron microscope(TEM) methods.The results indicate that the size distribution of nano-silver powder is narrow,average diameter size is 20~30nm,and polytropism structure under the CMC system;comparatively,the average diameter of nano-silver powder which prepared with the glucose system is 25~35nm,face-centered structure.Bacillus bacteria is one of advantage attached strain in the ocean,and the inhibition zone method was adopted in order to investigate the antimicrobial properties of nano-silver,the results show that nano-silver particles have excellent antimicrobial properties to marine bacteria.

【基金】 国家自然科学基金(50672090;50702053)
  • 【分类号】TB383.1
  • 【被引频次】24
  • 【下载频次】779
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