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烟草化学成分的气相色谱-质谱分析及尼古丁含量的测定

Analysis of Chemical Constituents of Tobacco by Gas Chromatography-Mass Spectrometry and Determination of Nicotine by Gas Chromatography

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【作者】 回瑞华侯冬岩李铁纯丛秀枝吴祎林

【Author】 HUI Rui-hua1,HOU Dong-yan1,LI Tie-chun1,CONG Xiu-zhi1,WU Wei-lin2(1.School of Chemistry and Life Science,Anshan Normal University,Anshan Liaoning 114007,China; 2.Shanxi University,Taiyuan Shanxi 030006,China)

【机构】 鞍山师范学院化学与生命科学学院山西大学

【摘要】 采用同时蒸馏萃取法与水蒸气蒸馏法提取烟草中挥发性成分并用气相色谱-质谱(GC/MS)法分别确认其化学成分,其中主要成分为尼古丁.用气相色谱法测定烟草中尼古丁的含量.尼古丁含量在0.446 4~0.892 8 mg/mL范围内与峰面积呈良好线性关系,回归方程为:A=61 670 M-2 894.8,相关系数为0.998 6,回收率为99.83%.

【Abstract】 Simultaneous distillation extraction method(SDE) and water distillation extraction method(WDE) are used for extracting the volatile chemical constituents of tobaccos and the chemical components are identified by gas chromatography/mass spectrometry(GC/MS) method respectively.Of them the major compound is nicotine.The contents of nicotine in tobaccos are determinated by gas chromatographic method.A good linear relationship between the concentrations in 0.446 4~0.892 8 mg/mL with peak area is found.The regression equation is A=61 670M-2 894.8 and correlation coefficient 0.998 6,the average recovery of the method is 99.83%.

【基金】 鞍山市重点科技项目(2009)
  • 【文献出处】 鞍山师范学院学报 ,Journal of Anshan Normal University , 编辑部邮箱 ,2011年06期
  • 【分类号】TS47;O657.63
  • 【被引频次】4
  • 【下载频次】563
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