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充氚不锈钢中氦泡长大行为的加热效应

Investigation of Temperature Effect on Helium Bubble Precipitation in HR-2 Stainless Steel

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【作者】 王小英申亮任大鹏陈向林陈丕恒姜桂芬刘婷婷

【Author】 WANG Xiao-ying1,SHEN Liang2,REN Da-peng2,CHEN Xiang-lin2, CHEN Pi-heng1,JIANG Gui-fen2,LIU Ting-ting1 (1.National Key Laboratory for Surface Physics and Chemistry,Mianyang621907,China; 2.China Academy of Engineering Physics,Mianyang621900,China)

【机构】 表面物理与化学国家重点实验室中国工程物理研究院

【摘要】 以室温贮存经历的充氚不锈钢试样为研究对象,计算了充氚不锈钢中氚、氦浓度的深度分布,利用透射电镜观察了充氚不锈钢在加热过程中氦泡的演化行为。结果表明:在氚压0.131MPa、780℃充氚8h后,不锈钢中氚在深度方向分布均匀,平均浓度为110μL/L;在空气室温环境下放置6a后,不锈钢中氚衰变的氦浓度在深度方向分布均匀,平均浓度为60μL/L;对充氚不锈钢加热处理后,在550℃/1h时效即可观察到氦泡;在950℃/1h和1050℃/1h时效时,氦泡明显长大,大的可达100nm,小的可达30nm,在晶界、晶内和位错处均可见氦泡。

【Abstract】 The influence of thermomechanical heat treatments,aging conditions (temperature and time) on helium bubble precipitation in tritiated HR-2 stainless steel was deal with.Helium was generated by the radioactive decay of tritium (tritium trick).The concentration distribution of tritium and 3 He in tritiated HR-2 stainless steel vessels was calculated based on diffusion and decay theories.The results show that concentration distribution of tritium is about 110μL/L homogeneous in depth during the storage of tritium at the pressure of 0.131MPa for 8hat 780℃,and the concentration distribution of helium is about 60μL/L homogeneous in depth later exposed to air for about 6a. The bubbles can be observed in the stainless steel aged at 550℃/1h.The large bubbles in grain boundaries and dislocation present aged at 950 ℃/1hand 1 050℃/1hand bubble dragging by dislocations toward the grain boundaries.The larger bubbles are about 100nm and the smaller bubbles are about 30nm in diameter.

【关键词】 充氚不锈钢时效氦泡
【Key words】 tritiated stainless steelaginghelium bubble
【基金】 表面物理与化学国家重点实验室开放基金资助项目(90000460200603)
  • 【文献出处】 原子能科学技术 ,Atomic Energy Science and Technology , 编辑部邮箱 ,2010年10期
  • 【分类号】TG142.71
  • 【被引频次】2
  • 【下载频次】124
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