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气相色谱法测定鸡蛋花药材中反式苦橙油醇的含量
Content determination of d-nerolidol in Mexican Frangipani by GC
【摘要】 目的:建立鸡蛋花药材中反式苦橙油醇的含量测定方法。方法:采用气相色谱内标法,以十四醇为内标,测定鸡蛋花药材中反式苦橙油醇的含量。结果:反式苦橙油醇在0.0363~0.7250mg/ml范围呈良好的线性关系(r=0.9999),平均加样回收率为100.4%,RSD=0.63%。结论:气相色谱法测定反式苦橙油醇的含量,准确度高且重复性好,可作为鸡蛋花药材的质量控制方法之一。
【Abstract】 Objective:To establish a method for the determination of d-nerolidol in Mexican Frangipani by GC.Methods:Tetradecyl alchohol served as the internal standard,GC method was used to determine the content of d-nerolidol in Mexican Frangipani.Results:The linear ranges of d-nerolidol was at 0.036 3-0.7250 mg/ml(r=0.999 9),the average recovery was 100.4% with a RSD of 0.63%.Conclusion:The method is accurate,reproducible,and can be used to control the quality of Mexican Frangipani.
【关键词】 鸡蛋花;
挥发油;
反式苦橙油醇;
气相色谱法;
含量测定;
【Key words】 Mexican Frangipani; Volatile oil; D-nerolidol; GC; Content determination;
【Key words】 Mexican Frangipani; Volatile oil; D-nerolidol; GC; Content determination;
- 【文献出处】 中国医药导报 ,China Medical Herald , 编辑部邮箱 ,2010年13期
- 【分类号】R284
- 【被引频次】7
- 【下载频次】176