【摘要】 目的建立附炎栓的质量标准。方法采用薄层色谱法对方中夏枯草、金银花进行定性鉴别,采用高效液相色谱法测定附炎栓中主要有效成分丹参酮ⅡA的含量。结果薄层色谱斑点清晰,专属性强,阴性对照无干扰。丹参酮ⅡA含量在10.096～50.48μg/mL范围内线性关系良好(r=0.999 5,n=5),平均回收率为98.19%,RSD=0.83%,(n=6)。结论该方法简便可靠,专属性强,重复性好,能较全面反映该制剂内在质量,可用于该制剂的质量控制。更多还原

【Abstract】 Objective To establish the quality standard of Fuyanshuan.Methods Prunella vulgaris and lonicera japonica in the preparation were qualitative identified by TLC.The main effective component tanshinone ⅡA was determined by HPLC.Results The spots of TLC were clear,with strong specificity and no negative interference.There was a good liner relationship of tanshinone ⅡA within the range of 10.096～50.48 μg/mL(r=0.999 5,n=5).The average recovery was 98.19%(RSD=0.83%,n=6).Conclusion The method was simple,accurate and reproducible.It can be used for the quality control of Fuyanshuan.更多还原