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草酸沉淀法合成自组装纳米Co3O4及性质
Synthesis and Characterizations of Self-assembled Nano Co3O4 by Oxalate-precipitation Method
【摘要】 <正>一维纳米材料具有高比表面积,表现出很多奇特的物理和化学性能,因此一维纳米材料的合成和性质引起了人们的广泛关注。目前,合成一维纳米氧化物的方法很多,如模板法合成一维纳米铁氧体、水热法合成γ-MnOOH纳米棒、静电纺丝法合
【Abstract】 A template-free route without adjusting the pH value of the system was suggested to synthesize self-assembled one-dimensional Co3O4 at room temperature.XRD,SEM,vibrating sample magnetometer(VSM) and cyclic voltammogram were used to investigate the crystal structure,morphologies,magnetic and electrical properties. Results show that the products are in pure cubic Co3O4 phase with a space group of Fd3m(227).The morphologies of all the synthesized samples are self-assembled nanorods or nanowires.The obtained Co3O4 shows paramagnetism at room temperature and good capacitive behavior in cyclic voltammetry curves.The influences of sintering temperature and sodium dodecyl sulfate(SDS) on the morphologies were also studied.
- 【文献出处】 无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,2010年03期
- 【分类号】TB383.1
- 【被引频次】13
- 【下载频次】348